2,6-Dibromo-benzamide synthesis
- Product Name:2,6-Dibromo-benzamide
- CAS Number:96237-91-1
- Molecular formula:C7H5Br2NO
- Molecular Weight:278.93
6575-12-8
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Yield:96237-91-1 92.6%
Reaction Conditions:
with sulfuric acid at 55;
Steps:
1.5; 2.5 (5) Amidation reaction:
Add 70 g of 2,6-dibromobenzonitrile to the reaction vessel and 250 mL of sulfuric acid. After the addition,The temperature is raised to about 55 degrees, and the reaction is kept for a period of time, followed by GC tracking until the reaction is complete.After the completion of the reaction, stir, cool, separate the ice water with water, filter with suction,Obtained 69 g of 2,6-dibromobenzamide with a content of 98% and a yield of 92.6%.
References:
CN111548276,2020,A Location in patent:Paragraph 0018; 0024; 0026; 0032
59870-37-0
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55-21-0
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$5.00/5G
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601-84-3
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$11.00/100mg
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