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ChemicalBook CAS DataBase List 2,6-Dichloroaniline
608-31-1

2,6-Dichloroaniline synthesis

14synthesis methods
-

Yield:608-31-1 80%

Reaction Conditions:

in water

Steps:

5 EXAMPLE 5
EXAMPLE 5 0.2 mole=41.2 g 3,5-dichloro-4-amino-benzoate were initially introduced into an autoclave together with 250 ml of water. The mixture was heated to 250° C. and stirred at this temperature for eight hours. The product was then recovered by steam distillation. 26 g of 2,6-dichloroaniline were obtained in a purity of 99.8%, corresponding to a yield of 80%.

References:

Bayer Aktiengesellschaft US5145958, 1992, A

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