2,6-DIMETHYL-NICOTINIC ACID synthesis
- Product Name:2,6-DIMETHYL-NICOTINIC ACID
- CAS Number:5860-71-9
- Molecular formula:C8H9NO2
- Molecular Weight:151.16
1122-43-6
126 suppliers
$9.00/100mg
5860-71-9
95 suppliers
$31.80/250mgs:
Yield:-
Steps:
Multi-step reaction with 2 steps
1: fluorosulfonyl fluoride; triethylamine / dichloromethane / 24 h / 20 °C / 760.05 Torr
2: bis(triphenylphosphine)nickel(II) chloride; 2.9-dimethyl-1,10-phenanthroline; manganese / N,N-dimethyl-formamide / 20 h / 20 °C / 760.05 Torr / Schlenk technique; Inert atmosphere; Glovebox
References:
Ma, Cong;Zhao, Chuan-Qi;Xu, Xue-Tao;Li, Zhao-Ming;Wang, Xiang-Yang;Zhang, Kun;Mei, Tian-Sheng [Organic Letters,2019,vol. 21,# 7,p. 2464 - 2467]
1721-13-7
62 suppliers
$149.00/250mg
5860-71-9
95 suppliers
$31.80/250mgs: