2-Acetyl-6-methoxynaphthalene synthesis
- Product Name:2-Acetyl-6-methoxynaphthalene
- CAS Number:3900-45-6
- Molecular formula:C13H12O2
- Molecular Weight:200.23
23981-80-8
174 suppliers
$8.00/1g
3900-45-6
403 suppliers
$10.00/10g
Yield:3900-45-6 72%
Reaction Conditions:
with (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile;N,N,N',N'-tetramethylguanidine in acetonitrile at 20; for 6 h;Irradiation;
Steps:
2.1 Experimental procedure for synthesis of 2a-2q
General procedure: To a 25 mL reaction tube, arylacetic acid (0.2 mmol), 4CzIPN (1 mol%), TMG (50 mol%) were dissolved in CH3CN (1.5 mL), and then the tube was stirred in air at room temperature for 6 h with the irradiation of 25 W blue LEDs. After reaction, the mixture was collected, and the residue was purified by column chromatography on silica gel to afford the desired products.
References:
He, Shuaiqi;Chen, Xiaolan;Zeng, Fanlin;Lu, Peipei;Peng, Yuyu;Qu, Lingbo;Yu, Bing [Chinese Chemical Letters,2020,vol. 31,# 7,p. 1863 - 1867] Location in patent:supporting information
129113-00-4
51 suppliers
$41.10/1g
3900-45-6
403 suppliers
$10.00/10g
84167-74-8
93 suppliers
$45.00/50mg
3900-45-6
403 suppliers
$10.00/10g
93-04-9
486 suppliers
$13.00/25g
75-36-5
577 suppliers
$17.92/100G
3900-45-6
403 suppliers
$10.00/10g
93-04-9
486 suppliers
$13.00/25g
108-24-7
0 suppliers
$14.00/250ML
3900-45-6
403 suppliers
$10.00/10g
58149-89-6
4 suppliers
inquiry