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32212-29-6

2-AMINO-N-ETHYLBENZAMIDE synthesis

11synthesis methods
-

Yield:32212-29-6 97%

Reaction Conditions:

in acetonitrile at 20 - 50; for 6 h;

Steps:



General procedure: A corresponding amine (20.2 mmol) was added to a solution ofisatoic anhydride (3.0 g, 18.4 mmol) in anhydrous MeCN(60 mL), and the mixture was stirred for 2 h at room temperature, then 4 h at 50 C. The solvent was evaporated to obtainamides

References:

Zaytsev;Revutskaya;Ku?menko;Novikov;Zubkov;Sorokina;Nikitina;Toze;Varlamov [Russian Chemical Bulletin,2015,vol. 64,# 6,p. 1345 - 1353][Izv. Akad. Nauk, Ser. Khim.,2015,# 6,p. 1345 - 1353,9]

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