2-BIPHENYLYL ISOCYANATE synthesis
- Product Name:2-BIPHENYLYL ISOCYANATE
- CAS Number:17337-13-2
- Molecular formula:C13H9NO
- Molecular Weight:195.22
90-41-5
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101-68-8
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$13.00/25g
17337-13-2
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$44.00/5g
Yield:17337-13-2 203.2 g
Reaction Conditions:
at 140 - 160; for 0.833333 h;Large scale;
Steps:
Preparation of 2-biphenyl isocyanate
Preparation of 2-biphenyl isocyanate
A three-neck flask with dropping funnel, precision glass stirrer and distillation attachment was initially charged with 1500 g of Desmodur 2460M and heated to 140° C.
Then, within 50 minutes, 243.7 g of 2-aminobiphenyl were added and the reaction temperature was kept below 160° C.
Subsequently, the product was distilled off under high vacuum (about 0.03 mbar), and 203.2 g of 2-biphenyl isocyanate, a clear liquid, were obtained.
References:
US2017/362165,2017,A1 Location in patent:Paragraph 0188
32315-10-9
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90-41-5
353 suppliers
$16.00/5g
17337-13-2
125 suppliers
$44.00/5g
![Methanesulfonic acid, 1,1,1-trifluoro-, [1,1'-biphenyl]-2-yl ester](/CAS/20200611/GIF/17763-65-4.gif)
17763-65-4
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917-61-3
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17337-13-2
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$44.00/5g
947-84-2
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17337-13-2
125 suppliers
$44.00/5g
