2-BROMO-3-CHLOROPHENOL synthesis
- Product Name:2-BROMO-3-CHLOROPHENOL
- CAS Number:855836-62-3
- Molecular formula:C6H4BrClO
- Molecular Weight:207.45
108-43-0
301 suppliers
$13.00/5g
855836-62-3
100 suppliers
$57.50/250 mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C
1.2: 87 percent / hexane; tetrahydrofuran / 36 h / Heating
2.1: s-BuLi; TMEDA / cyclohexane; hexane; tetrahydrofuran / 2 h / -78 °C
2.2: 64 percent / 1,2-dibromoethane / tetrahydrofuran; hexane; cyclohexane / -78 - 20 °C
3.1: 82 percent / NaOH / ethanol / Heating
References:
Sanz, Roberto;Castroviejo, M. Pilar;Fernandez, Yolanda;Fananas, Francisco J. [Journal of Organic Chemistry,2005,vol. 70,# 16,p. 6548 - 6551]
863870-78-4
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855836-62-3
100 suppliers
$57.50/250 mg
108-43-0
301 suppliers
$13.00/5g
89284-48-0
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13659-23-9
188 suppliers
$19.00/1g
13631-21-5
208 suppliers
$6.00/1g
855836-62-3
100 suppliers
$57.50/250 mg
108-43-0
301 suppliers
$13.00/5g
40979-03-1
1 suppliers
inquiry
13659-23-9
188 suppliers
$19.00/1g
13631-21-5
208 suppliers
$6.00/1g
855836-62-3
100 suppliers
$57.50/250 mg
108-43-0
301 suppliers
$13.00/5g
13659-23-9
188 suppliers
$19.00/1g
13631-21-5
208 suppliers
$6.00/1g
855836-62-3
100 suppliers
$57.50/250 mg