2-BROMO-N,N-DIETHYLETHYLAMINE HYDROBROMIDE synthesis
- Product Name:2-BROMO-N,N-DIETHYLETHYLAMINE HYDROBROMIDE
- CAS Number:5392-81-4
- Molecular formula:C6H14BrN
- Molecular Weight:180.09
1069-72-3
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Yield:-
Reaction Conditions:
with water;sodium carbonate in ethyl acetate;
Steps:
70
Example 70; 109: 2-Bromo-N,N-diethylethylamine hydrobromide is commercially available and the salt must be freed prior to addition by stirring the reagent in sat. Na2CO3 and EtOAc (1:1) and extracting the freed amine into the organic layer. Otherwise, the compound was made in a similar fashion as compound 107, however the desired product was not purified by silica gel chromatography, instead isolated as the crude product 109 (50 mg): MS: 635 (M+1).
References:
US2008/58315,2008,A1 Location in patent:Page/Page column 61
100-37-8
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