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346695-08-7

2-Bromo-N-propylbenzamide synthesis

3synthesis methods
-

Yield:346695-08-7 91%

Reaction Conditions:

Stage #1: 2-bromobenzoic-acidwith triethylamine;isobutyl chloroformate in dichloromethane; for 0.25 h;Inert atmosphere;Schlenk technique;
Stage #2: propylamine in dichloromethane at 0;

References:

Liu, Hailong;Han, Weibiao;Li, Chun;Ma, Zhiyong;Li, Ruixiang;Zheng, Xueli;Fu, Haiyan;Chen, Hua [European Journal of Organic Chemistry,2016,vol. 2016,# 2,p. 389 - 393] Location in patent:supporting information

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