2-BROMOPHENYLACETYL CHLORIDE synthesis
- Product Name:2-BROMOPHENYLACETYL CHLORIDE
- CAS Number:55116-09-1
- Molecular formula:C8H6BrClO
- Molecular Weight:233.49
18698-97-0
343 suppliers
$10.00/1g
55116-09-1
36 suppliers
$865.55/5ML
Yield:55116-09-1 92%
Reaction Conditions:
with oxalyl dichloride;N,N-dimethyl-formamide in dichloromethane at 0 - 30; for 2 h;Reagent/catalyst;Solvent;Temperature;
Steps:
2-8
At 0 °C, oxalyl chloride (30 mmol, 2.54 mL) was added to 2-bromophenylacetic acid (30 mmol, 6.45 g) dissolved in DCM (30 mL), then 0.6 g of DMF was added, and the reaction was performed at 30 °C for 2 h. After completion, rotary evaporation was carried out at 35°C to obtain compound 1 (10.3 g, 92%).
References:
CN114751860,2022,A Location in patent:Paragraph 0151-0155; 0161-0164; 0170-0173; 0179-0182; ...
4870-65-9
195 suppliers
$8.00/1g
55116-09-1
36 suppliers
$865.55/5ML
57486-69-8
146 suppliers
$6.00/1g
55116-09-1
36 suppliers
$865.55/5ML