2-Butanone, 1,1-diethoxy- synthesis

7synthesis methods

Product Name:2-Butanone, 1,1-diethoxy-
CAS Number:6136-92-1
Molecular formula:C8H16O3
Molecular Weight:160.21

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: bis(trichloromethyl) carbonate; triethylamine / dichloromethane / 2 h / 0 - 20 °C
2: tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

References:

Ayala-Mata, Francisco;Barrera-Mendoza, Citlalli;Jimenez-Vazquez, Hugo A.;Vargas-Diaz, Elena;Zepeda, L. Gerardo [Molecules,2012,vol. 17,# 12,p. 13864 - 13878]

2,2-DIETHOXY-N-METHOXY-N-METHYLACETAMIDE

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811-49-4
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References

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925-90-6 Synthesis

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References

2386-64-3
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6065-82-3
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References

6065-82-3
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References

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2-Butanone, 1,1-diethoxy- synthesis