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2-Butenoic acid, 3-(3-fluorophenyl)-, (E)- (9CI) synthesis

1synthesis methods

455-36-7 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 3 h / 0 °C
1.2: 20 °C
2.1: sodium hydroxide / ethanol / 20 °C

References:

Yan, Qiaozhi;Kong, Duanyang;Zhao, Wei;Zi, Guofu;Hou, Guohua [Journal of Organic Chemistry,2016,vol. 81,# 5,p. 2070 - 2077]

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