2-CARBOXY-3-CARBOXYMETHYLQUINOLINE synthesis
- Product Name:2-CARBOXY-3-CARBOXYMETHYLQUINOLINE
- CAS Number:132623-44-0
- Molecular formula:C12H9NO4
- Molecular Weight:231.2
53821-46-8
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132623-44-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 22 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 20 h / Heating
2: 66 percent / methanol / 1.) RT, 15 h, 2.) reflux, 2 h
3: 45 percent / 6 N aq. HCl / 4 h
References:
Gray, Nancy M.;Dappen, Michael S.;Cheng, Brian K.;Cordi, Alexis A.;Biesterfeldt, John P.;et al. [Journal of Medicinal Chemistry,1991,vol. 34,# 4,p. 1283 - 1292]
54934-04-2
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132623-44-0
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