2-CHLOROBENZANILIDE synthesis
- Product Name:2-CHLOROBENZANILIDE
- CAS Number:6833-13-2
- Molecular formula:C13H10ClNO
- Molecular Weight:231.68
609-65-4
342 suppliers
$21.00/25g
6833-13-2
39 suppliers
$50.00/250mg
Yield:6833-13-2 98%
Reaction Conditions:
with triethylamine hydrochloride;triethylamine in chloroform;water;benzene;
Steps:
I Preparation of 2-chlorobenzoyl anilide
EXAMPLE I Preparation of 2-chlorobenzoyl anilide Fourth and seven-tenths grams (4.7 g) (0.05 mole) anilide and 5.10 g triethylamine are mixed in 150 milliliters (ml) of benzene by stirring. A solution of 8.75 g (0.05 mole) 2-chlorobenzoyl chloride in 50 ml chloroform is added to the first mixture through a dropping funnel. An exothermic reaction takes place. After the addition is finished, the mixture is refluxed for 1/2 hour. The mixture is cooled with the product solidifying. The product is filtered, added to water, and stirred to dissolve triethylamine hydrochloride. The product is filtered again and dried to yield 11.3 g of the desired product (98% yield) m.p. 115°-117° C.
References:
US4390549,1983,A
609-65-4
342 suppliers
$21.00/25g
62-53-3
680 suppliers
$10.00/1g
6833-13-2
39 suppliers
$50.00/250mg
89-98-5
681 suppliers
$15.00/25g
62-53-3
680 suppliers
$10.00/1g
6833-13-2
39 suppliers
$50.00/250mg
62-53-3
680 suppliers
$10.00/1g
118-91-2
680 suppliers
$14.00/25g
6833-13-2
39 suppliers
$50.00/250mg
118-91-2
680 suppliers
$14.00/25g
6833-13-2
39 suppliers
$50.00/250mg