2-CHLOROPHENYLZINC IODIDE synthesis
- Product Name:2-CHLOROPHENYLZINC IODIDE
- CAS Number:148651-35-8
- Molecular formula:C6H4ClIZn
- Molecular Weight:303.84
615-41-8
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$5.00/1g
7440-66-6
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$14.00/5g
148651-35-8
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$216.00/50ml
Yield:148651-35-8 96%
Reaction Conditions:
with water in further solvent(s);byproducts: C6H5Cl; Sonication; (N2); solvent = 1,1,3,3-tetramethylurea contg. water; 2 equivs. of Zn powder used; 30 °C, ultrasound applied for 8 h; 100% conversion; not isolated; conversion and yield detd. by quenching with I2;
References:
Takagi, Kentaro [Chemistry Letters,1993,# 3,p. 469 - 472]