2-ETHOXY-TRIETHYLPHOSPHONOACETATE synthesis
- Product Name:2-ETHOXY-TRIETHYLPHOSPHONOACETATE
- CAS Number:13676-06-7
- Molecular formula:C10H21O6P
- Molecular Weight:268.24
Yield:13676-06-7 100%
Reaction Conditions:
at 50; for 3 h;
Steps:
20.d.2 d. 2: Ethyl (diethoxyphosphoryl) ethoxyacetate
36.3 g (218 mmol) of ethyl chloroethoxy- acetate and 37.4 ml (218 mmol) of triethyl phosphite are heated at 50oC for 3 hours. The reaction medium is evaporated to dryness under vacuum. 57 g (100%) of crude ethyl (diethoxyphosphoryl) ethoxyacetate are obtained.
References:
WO2004/113331,2004,A1 Location in patent:Page 92-93
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