2-Ethylhexyl chloroformate synthesis
- Product Name:2-Ethylhexyl chloroformate
- CAS Number:24468-13-1
- Molecular formula:C9H17ClO2
- Molecular Weight:192.68
Yield:-
Steps:
1
Example 1; A polyvinyl chloride was prepared in accordance with the process of the invention comprising the steps of: -Vinyl chloride monomer (VCM) is produced from ethylene and chlorine in a process as described in ref. [1]. - CO is prepared by reduction of C02 in a process as described in ref. [2]. - Phosgene is prepared from chlorine and CO in a process as described in ref. [3]. The CO is obtained as described above, the chlorine is available from a chlorine-handling facility on site. - The phosgene produced in the previous step and 2-ethylhexanol were immediately used to prepare 2-Ethylhexyl chloroformate according to the process described in ref. [4]. - 2-Ethylhexyl chloroformate of the previous step is used together with hydrogen peroxide and aqueous sodium hydroxide to prepare di (2- ethylhexyl) peroxydicarbonate in a process as described in ref. [5]. -Di (2-ethylhexyl) peroxydicarbonate of the previous step is used as initiator in a suspension polymerization process as described in ref. [6] to produce polyvinyl chloride (PVC) from VCM.
References:
AKZO NOBEL N.V. WO2005/75419, 2005, A1 Location in patent:Page/Page column 14
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