2-HYDROXY-4,6-DIMETHOXYBENZOIC ACID synthesis
- Product Name:2-HYDROXY-4,6-DIMETHOXYBENZOIC ACID
- CAS Number:3187-19-7
- Molecular formula:C9H10O5
- Molecular Weight:198.17
500-99-2
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3187-19-7
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 97 percent / 3 h / 110 °C
2.1: 90 percent / NBS / CH2Cl2 / 1 h / 0 °C
3.1: 67 percent / KOH / methanol / 2.5 h / 20 °C
4.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / -25 °C
4.2: 65 percent / tetrahydrofuran; CH2Cl2 / 20 °C
References:
Runge;Haufe [Journal of Organic Chemistry,2000,vol. 65,# 25,p. 8737 - 8742]
500-99-2
295 suppliers
$10.00/1g
124-38-9
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$214.00/14L
3187-19-7
61 suppliers
$73.79/1g
23133-74-6
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3187-19-7
61 suppliers
$73.79/1g