2-Iodobenzyl chloride synthesis
- Product Name:2-Iodobenzyl chloride
- CAS Number:59473-45-9
- Molecular formula:C7H6ClI
- Molecular Weight:252.48
5159-41-1
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59473-45-9
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Yield: 89%
Reaction Conditions:
with thionyl chloride in tetrahydrofuran at 0 - 20;
Steps:
2-Iodobenzyl Chloride (2e)
Prepared in the same manner as described for 2b, using 2-iodobenzylalcohol (1.17 g, 5 mmol), which afforded 2e; yield: 1.12 g (89%);white solid.1H NMR (400 MHz, CDCl3): δ = 7.84 (d, J = 7.9 Hz, 1 H), 7.46 (d, J = 7.7Hz, 1 H), 7.34 (t, J = 7.6 Hz, 1 H), 6.99 (t, J = 7.7 Hz, 1 H), 4.66 (s, 2 H). 13C NMR (100 MHz, CDCl3): δ = 51.2, 99.7, 129.0, 130.2, 130.3, 139.9,140.0.
References:
Bedford, Robin B.;Gallagher, Timothy;Pye, Dominic R.;Savage, William [Synthesis,2015,vol. 47,# 12,art. no. SS-2014-C0739-ST,p. 1761 - 1765]
10175-33-4
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183789-20-0
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59473-45-9
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