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ChemicalBook CAS DataBase List 2-Methyl-5-nitrobenzenesulfonyl chloride
121-02-8

2-Methyl-5-nitrobenzenesulfonyl chloride synthesis

3synthesis methods
Add 6.90 g (0.05 mol) of p-nitrotoluene to a 100 mL three-necked flask, slowly add 17.5 g (0.15 mol) of chlorosulfonic acid dropwise with vigorous stirring, and after dropping, warm up the reaction to 65°C for 24 h. After the reaction, the reaction soluti
-

Yield: 100%

Reaction Conditions:

with chlorosulfonic acid

References:

Tagiev;Kazaz;Anyl [Russian Journal of Applied Chemistry,2012,vol. 85,# 10,p. 1581 - 1585][Zh. Prikl. Khim. (S.-Peterburg, Russ. Fed.),2012,vol. 85,# 10,p. 1648 - 1652,5]

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