2-Methylcyclohexanone synthesis
- Product Name:2-Methylcyclohexanone
- CAS Number:583-60-8
- Molecular formula:C7H12O
- Molecular Weight:112.17
74-88-4
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$15.00/10g
583-60-8
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$10.00/1g
Yield:583-60-8 95%
Reaction Conditions:
Stage #1:cyclohexanone with bis(trimethylsilyl)amidomagnesium chloride lithium chloride complex at 0; for 0.0833333 h;
Stage #2:methyl iodide
Steps:
The preparation of the bis(trimethylsilyl) amide 33 can be achieved by reacting bis(trimethylsilyl)amine with i-PrMgCl·LiCl at room temperature (see Scheme 5). This base can efficiently be used to deprotonate ketones like e.g. cyclohexanone as can be seen from Scheme 5.
References:
Ludwig-Maximilians-Universit?t München EP1810974, 2007, A1 Location in patent:Page/Page column 6
583-59-5
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583-60-8
188 suppliers
$10.00/1g
1122-26-5
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$119.00/500mg
583-60-8
188 suppliers
$10.00/1g
