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ChemicalBook CAS DataBase List 2-Methanesulfonyl-4,6-dimethoxypyrimidine
113583-35-0

2-Methanesulfonyl-4,6-dimethoxypyrimidine synthesis

4synthesis methods
One method for preparing 2-Methanesulfonyl-4,6-dimethoxypyrimidine comprises with 4, 6-dihydroxyl-2-methylthiopyrimidine is a main raw material, and through superchlorination, methoxylation and oxidizing reaction, reaction formula is as follows:
2-Methanesulfonyl-4,6-dimethoxypyrimidine synthesis
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: methanol / 25 °C
2: 3-chloroperoxybenzoic acid / CH2Cl2 / 5 h / 30 °C

References:

Zhang, Jing;Zhang, Li;Zhou, Ying;Guo, Yin-Long [Journal of Mass Spectrometry,2007,vol. 42,# 11,p. 1514 - 1521]

FullText

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