2-NITROPROPENE synthesis

10synthesis methods

Product Name:2-NITROPROPENE
CAS Number:4749-28-4
Molecular formula:C3H5NO2
Molecular Weight:87.08

2-Nitro-1-propene is prepared by dehydration of 2-nitro-1-propanol (ca. 98% purity commercially or prepared from Nitroethane and formalin, yield 70%) with phthalic anhydride (73%) or Acetic Anhydride-AcONa (85%).

1-Propen-2-amine, N,N-bis[(trimethylsilyl)oxy]-

102588-22-7
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4749-28-4
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Yield:4749-28-4 95 % Spectr.

Reaction Conditions:

with bromine;tetrabutylammonium acetate in dichloromethane at -78 - 20;

References:

Kunetsky, Roman A.;Dilman, Alexander D.;Struchkova, Marina I.;Tartakovsky, Vladimir A.;Ioffe, Sema L. [Tetrahedron Letters,2005,vol. 46,# 31,p. 5203 - 5205]

2902-96-7
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$29.00/5G

4749-28-4
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References

2425-66-3 Synthesis

2425-66-3
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4749-28-4
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References

79-46-9 Synthesis

79-46-9
200 suppliers
$10.00/5G

108-03-2
174 suppliers
$10.00/5g

4749-28-4
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3156-70-5
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References

609-31-4
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4749-28-4
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References

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2-NITROPROPENE synthesis

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