2-Phenylacryloyl chloride synthesis
- Product Name:2-Phenylacryloyl chloride
- CAS Number:51491-68-0
- Molecular formula:C9H7ClO
- Molecular Weight:166.6
101-41-7
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$15.00/25mL
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium carbonate; tetra-(n-butyl)ammonium iodide / toluene / 12 h / 50 °C
2: sodium hydroxide / 2 h / Reflux
3: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere
References:
Kong, Wangqing;Wang, Qian;Zhu, Jieping [Angewandte Chemie - International Edition,2017,vol. 56,# 14,p. 3987 - 3991][Angew. Chem.,2017,vol. 129,# 14,p. 4045 - 4049]
492-38-6
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$10.00/1g
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103-82-2
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$22.19/5g
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1865-29-8
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$31.00/100mg
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529-64-6
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$70.39/25 g
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