2-(Thiocyanatomethylthio)benzothiazole synthesis
- Product Name:2-(Thiocyanatomethylthio)benzothiazole
- CAS Number:21564-17-0
- Molecular formula:C9H6N2S3
- Molecular Weight:238.35
The 2-mercaptobenzothiazole was used as a raw material, and 2-chloromethylthiobenzothiazole was obtained by chloromethylation, and then phenothiocyanine (phenothiocyanine) was further obtained according to the second synthetic step of the first method.
3507-54-8
4 suppliers
inquiry
21564-17-0
220 suppliers
$163.00/25mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1: 28 percent / p-nitrobenzoyl chloride / CH2Cl2 / 1 h / 50 °C
2: 80 percent / aq. benzyltriethylammonium chloride / 10 h / 90 °C
References:
Muthusubramanian, Lakshmi;Mitra, Rajat B.;Sundara Rao;Raghavan [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1996,vol. 35,# 12,p. 1331 - 1334]
![2-[(chloromethyl)thio]benzothiazole](/CAS/GIF/28908-00-1.gif)
28908-00-1
11 suppliers
inquiry
540-72-7
476 suppliers
$13.50/100G
21564-17-0
220 suppliers
$163.00/25mg
149-30-4
689 suppliers
$5.00/25g
21564-17-0
220 suppliers
$163.00/25mg
615-22-5
188 suppliers
$10.00/5g
21564-17-0
220 suppliers
$163.00/25mg
3268-79-9
58 suppliers
$24.00/5g
149-30-4
689 suppliers
$5.00/25g
21564-17-0
220 suppliers
$163.00/25mg