ChemicalBook CAS DataBase List 2-UNDECENOIC ACID

2-UNDECENOIC ACID synthesis

8synthesis methods

Product Name:2-UNDECENOIC ACID
CAS Number:15790-94-0
Molecular formula:C11H20O2
Molecular Weight:184.28

2-Undecenoic acid is an organic intermediate that has been reported in the literature to be prepared in one step by nonanal and diethyl methyl phosphonoacetate or by oxidation of undecanoic acid.

638-53-9
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15790-94-0
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: Zn(2,2,6,6-tetramethylpiperidine)_2*2LiCl; zinc(II) chloride / tetrahydrofuran / 1.5 h / -40 °C / Inert atmosphere; Sealed tube
1.2: 12 h / -40 - 60 °C / Inert atmosphere; Sealed tube
2.1: ozone / acetone / 1 h / -78 °C / Inert atmosphere
2.2: 5 h / 0 - 20 °C / Inert atmosphere
3.1: Zn(2,2,6,6-tetramethylpiperidine)_2*2LiCl; zinc(II) chloride / tetrahydrofuran / 1.5 h / -40 °C / Inert atmosphere; Sealed tube
3.2: 12 h / -40 - 60 °C / Inert atmosphere; Sealed tube

References:

Zhao, Yizhou;Chen, Yifeng;Newhouse, Timothy R. [Angewandte Chemie - International Edition,2017,vol. 56,# 42,p. 13122 - 13125][Angew. Chem.,2017,vol. 129,# 42,p. 13302 - 13305,4]

112-37-8
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15790-94-0
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References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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15790-94-0
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References

124-19-6 Synthesis

124-19-6
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141-82-2 Synthesis

141-82-2
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15790-94-0
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References

124-19-6 Synthesis

124-19-6
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$7.00/25g

141-82-2 Synthesis

141-82-2
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$5.00/25g

15790-94-0
51 suppliers
$31.39/1g

References

2-UNDECENOIC ACID Related Search:

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2-UNDECENOIC ACID synthesis

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