ChemicalBook CAS DataBase List 2,4(1H,3H)-Pyrimidinedione, 1-methyl-5-(trifluoromethyl)-

2,4(1H,3H)-Pyrimidinedione, 1-methyl-5-(trifluoromethyl)- synthesis

3synthesis methods

Product Name:2,4(1H,3H)-Pyrimidinedione, 1-methyl-5-(trifluoromethyl)-
CAS Number:21579-18-0
Molecular formula:C6H5F3N2O2
Molecular Weight:194.11

615-77-0 Synthesis

615-77-0
136 suppliers
$34.00/100mg

2314-97-8 Synthesis

2314-97-8
186 suppliers
$40.00/25g

2,4(1H,3H)-Pyrimidinedione, 1-methyl-5-(trifluoromethyl)-

21579-18-0
6 suppliers
inquiry

Yield:21579-18-0 77%

Reaction Conditions:

with caesium carbonate in dimethyl sulfoxide at 20; for 24 h;Schlenk technique;Inert atmosphere;Irradiation;

References:

Huang, Yang;Lei, Yun-Yun;Zhao, Liang;Gu, Jiwei;Yao, Qiuli;Wang, Ze;Li, Xiao-Fei;Zhang, Xingang;He, Chun-Yang [Chemical Communications,2018,vol. 54,# 97,p. 13662 - 13665] Location in patent:supporting information

615-77-0 Synthesis

615-77-0
136 suppliers
$34.00/100mg

tert-butyl 2-[(trifluoromethyl)sulfonyl]hydrazinecarboxylate

56572-25-9
0 suppliers
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21579-18-0
6 suppliers
inquiry

References

2,4(1H,3H)-Pyrimidinedione, dihydro-1-methyl-5-(trifluoromethyl)-

85199-74-2
0 suppliers
inquiry

21579-18-0
6 suppliers
inquiry

References

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2,4(1H,3H)-Pyrimidinedione, 1-methyl-5-(trifluoromethyl)- synthesis