2-Quinolinecarboxaldehyde,5,6,7,8-tetrahydro-8-oxo-(9CI) synthesis
- Product Name:2-Quinolinecarboxaldehyde,5,6,7,8-tetrahydro-8-oxo-(9CI)
- CAS Number:238755-38-9
- Molecular formula:C10H9NO2
- Molecular Weight:175.18
91-63-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: 98 percent / H2; TFA / 10percent Pd/C / 60 h / 20 °C
2.1: 79 percent / Ac2O / 120 h / 150 - 160 °C
3.1: O3 / CH2Cl2; methanol / -77 °C
3.2: 89 percent / Me2S / CH2Cl2; methanol / -77 - 20 °C
References:
Bell, Thomas W.;Khasanov, Alisher B.;Drew, Michael G. B. [Journal of the American Chemical Society,2002,vol. 124,# 47,p. 14092 - 14103]
2617-98-3
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238755-38-9
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