3-(2-METHOXY-PHENYLAMINO)-PROPIONITRILE synthesis
2synthesis methods
- Product Name:3-(2-METHOXY-PHENYLAMINO)-PROPIONITRILE
- CAS Number:27472-15-7
- Molecular formula:C10H12N2O
- Molecular Weight:176.22
Yield:27472-15-7 93%
Reaction Conditions:
Stage #1: 2-methoxy-phenylaminewith potassium tert-butylate;1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazolium chloride;copper(l) chloride in toluene; for 0.333333 h;Inert atmosphere;Michael Addition;
Stage #2: acrylonitrile in toluene at 22; for 15 h;Inert atmosphere;Michael Addition;
References:
Kim, Seongcheol;Kang, Seongil;Kim, Gihyeon;Lee, Yunmi [Journal of Organic Chemistry,2016,vol. 81,# 10,p. 4048 - 4057]
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