3,3-Dimethylbutyric acid synthesis
- Product Name:3,3-Dimethylbutyric acid
- CAS Number:1070-83-3
- Molecular formula:C6H12O2
- Molecular Weight:116.16
2987-16-8
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Yield:1070-83-3 95%
Reaction Conditions:
with oxygen;copper(II) acetate monohydrate;cobalt(II) diacetate tetrahydrate in water at 20; under 760.051 Torr; for 3 h;
Steps:
18 Example 18 Oxidation of 3,3-dimethylbutyraldehyde to produce 3,3-dimethylbutyric acid
Under normal pressure oxygen, water (2mL), 3,3-dimethylbutyraldehyde (1mmol), Cu(OAc)2· H2O (0.0001mmol, 0.01% mole fraction) and Co(OAc)2.4H2O (0.0001 mmol, 0.01% mole fraction) was added to a 15 mL glass reaction tube, and an oxygen balloon was connected.The reaction tube was placed in a 20°C water bath and the reaction was stirred for 3 hours. After the reaction was completed, the target product was obtained by extraction, concentration, and drying to constant weight. The separation yield was 95%, and the product was a colorless liquid.T
References:
CN111116348,2020,A Location in patent:Paragraph 0046-0047
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