3-(4-BROMOPHENYL)-2-CHLOROQUINOLINE synthesis
- Product Name:3-(4-BROMOPHENYL)-2-CHLOROQUINOLINE
- CAS Number:85274-82-4
- Molecular formula:C15H9BrClN
- Molecular Weight:318.6
![Formamide, N-[2-[2-(4-bromophenyl)ethynyl]phenyl]-](/CAS/20210305/GIF/1200688-13-6.gif)
1200688-13-6
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85274-82-4
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$265.00/250mg
Yield:85274-82-4 99%
Reaction Conditions:
Stage #1: C15H10BrNOwith N-ethyl-N,N-diisopropylamine;trichlorophosphate in dichloromethane at 0;Inert atmosphere;
Stage #2: with tetrabutyl-ammonium chloride in dichloromethane at 40; for 15 h;Inert atmosphere;
References:
Liu, Lanying;Wang, Yong;Wang, Honggen;Peng, Changlan;Zhao, Jiaji;Zhu, Qiang [Tetrahedron Letters,2009,vol. 50,# 48,p. 6715 - 6719] Location in patent:experimental part