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ChemicalBook CAS DataBase List 3,5-DIBROMO-2-METHYLTHIOPHENE
29421-73-6

3,5-DIBROMO-2-METHYLTHIOPHENE synthesis

6synthesis methods
At zero temperature, 120.0 mL of glacial acetic acid was used to dissolve the compound of formula 6, 2-methylthiophene (24.50 g, 250.00 mmol), and then placed into a 250.0 mL single-necked flask, and under rapid stirring, 30.0 mL of a mixture of liquid br
-

Yield: 99.7%

Reaction Conditions:

with bromine;acetic acid at 20;

References:

Jia, Chuancheng;Wang, Jinying;Yao, Changjiang;Cao, Yang;Zhong, Yuwu;Liu, Zhirong;Liu, Zhongfan;Guo, Xuefeng [Angewandte Chemie - International Edition,2013,vol. 52,# 33,p. 8666 - 8670][Angew. Chem.,2013,vol. 125,# 33,p. 8828 - 8832,5] Location in patent:supporting information

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