3-Vinylaniline synthesis
- Product Name:3-Vinylaniline
- CAS Number:15411-43-5
- Molecular formula:C8H9N
- Molecular Weight:119.16
54060-30-9
534 suppliers
$8.00/5g
15411-43-5
113 suppliers
$26.00/100mg
587-02-0
178 suppliers
$10.00/1g
Yield:-
Reaction Conditions:
with carbon monoxide;hydrogen in tetrahydrofuran at 70; under 7757.43 Torr; for 6 h;Autoclave;
Steps:
2.3. General experimental procedure for synthesis of alkenes viasemi-hydrogenation of alkynes
General procedure: To a 100 mL high-pressure reactor, phenylacetylene (1 mmol),Pd (0.96 mol%) in a 10 mL THF were transferred under an inertatmosphere. The reactor was flushed three times with nitrogen then pressurized with desired 150 psi of syngas, then heated at70C with constant stirring (400 rpm) for 6 h. After the comple-tion of reaction, the reactor cooled down to room temperature andthe remaining syngas was carefully depressurized. The resultantreaction mixture filtered off by simple filtration. The filtrate was then collected in sample vial and the product was extracted for fur-ther analysis such as GC, GC-MS,1H &13C NMR and matched with those of authentic data. Selective experiments were performed in triplicate and it was observed that results showed variation of ±2%.
References:
Jagtap, Samadhan A.;Sasaki, Takehiko;Bhanage, Bhalchandra M. [Journal of Molecular Catalysis A: Chemical,2016,vol. 414,p. 78 - 86]
586-39-0
99 suppliers
$131.00/2.5g
15411-43-5
113 suppliers
$26.00/100mg
586-39-0
99 suppliers
$131.00/2.5g
15411-43-5
113 suppliers
$26.00/100mg
587-02-0
178 suppliers
$10.00/1g
54060-30-9
534 suppliers
$8.00/5g
15411-43-5
113 suppliers
$26.00/100mg
586-39-0
99 suppliers
$131.00/2.5g
7369-50-8
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15411-43-5
113 suppliers
$26.00/100mg