3-CHLOROPROPYL PHENYL SULFIDE synthesis
- Product Name:3-CHLOROPROPYL PHENYL SULFIDE
- CAS Number:4911-65-3
- Molecular formula:C9H11ClS
- Molecular Weight:186.7
Yield:4911-65-3 100%
Reaction Conditions:
with triethylamine in tetrahydrofuran at 25; for 12 h;
Steps:
R Procedure R
Procedure R [(3-CHLOROPROPYL)SULFANYL]BENZENE: A mixture of benzenethiol (0.550 9, 5.00 mmol), 1-bromo-3-chloropropane (106 mg, 5.50 mmol), TEA (1.01 g, 10.0 mmol) and THF (10.0 ML) was stirred for 12 h at 25° C. The resulting crude mixture was diluted with water (40 ML), the aqueous layer was extracted with CH2Cl2 (3*30 ML).. The combined organic layers were concentrated in vacuo and the residue was purified by preparative TLC using hexane:EtOAc (10:1) to give the desired product [(3-chloropropyl)sulfanyl]benzene (1.05 g, 100%)..
References:
US6727264,2004,B1 Location in patent:Page column 138; 139
24536-40-1
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$45.00/10mg
4911-65-3
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$73.90/5g
108-98-5
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107-05-1
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$16.80/100ML
5296-64-0
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$29.00/5g
4911-65-3
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$73.90/5g
