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ChemicalBook CAS DataBase List 3-IODOTHIOPHENE
10486-61-0

3-IODOTHIOPHENE synthesis

12synthesis methods
In a 100 mL reactor, 8.04 g (0.049t001) of 3-bromothiophene, 0.47 g (2.5 mm01) of CuI, 0.43 g (4.9ret001) of N,N'-dimethylethylenediamine, 16.27 g (0.098m01) of I(I, and 20 mL of n-butanol were added to a 100 mL reactor, and the reaction was carried out b
-

Yield: 71%

Reaction Conditions:

with N-iodo-succinimide in acetonitrile at 25; for 14 h;

References:

Thiebes, Christoph;Prakash, G. K. Surya;Petasis, Nicos A.;Olah, George A. [Synlett,1998,# 2,p. 141 - 142]

188290-36-0 Synthesis
Thiophene(SIV) (9CI)

188290-36-0
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