3-METHYLPENTANE-1,3,5-TRIOL synthesis
- Product Name:3-METHYLPENTANE-1,3,5-TRIOL
- CAS Number:7564-64-9
- Molecular formula:C6H14O3
- Molecular Weight:134.17
105-50-0
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: 92 percent / BF3*Et2O / CH2Cl2 / 6 h / Ambient temperature
2: 90 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating
3: 100 percent / p-toluenesulphonic acid / CH2Cl2 / 4 h / 0 °C
4: 96 percent / CaCO3, HgCl2 / acetonitrile; H2O / 1 h / Ambient temperature
5: 1) Mg / 1) ether, 2) 0 deg C, 15 min
6: 90 percent / p-toluenesulphonic acid / methanol / 4 h / Heating
References:
Chakraborty, T. K.;Bhushan, Vidya;Chandrasekaran, S. [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,1983,vol. 22,# 1,p. 9 - 11]
674-26-0
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503-49-1
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$35.00/25mg
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19115-49-2
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$130.00/100mg
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56652-39-2
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7564-64-9
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