3'-OMe-2-NH2-A synthesis
- Product Name:3'-OMe-2-NH2-A
- CAS Number:80791-88-4
- Molecular formula:C11H16N6O4
- Molecular Weight:296.28
118-00-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) hexamethyldisilazane, chlorotrimethylsilane; 2.) hexamethyldisilazane, CF3SO3SiMe3, NH3 / 1.) reflux, 16 h; 2.) 150 deg C, 3 d (sealed bomb)
2: 47 percent / SnCl2*2H2O / dimethylformamide; 1,2-dimethoxy-ethane / 50 °C
References:
Robins, Morris J.;Hansske, Fritz;Bernier, Salwa E. [Canadian Journal of Chemistry,1981,vol. 59,p. 3360 - 3364]