2-[(2-ethoxyphenoxy)methyl]morpholine hydrochloride synthesis
- Product Name:2-[(2-ethoxyphenoxy)methyl]morpholine hydrochloride
- CAS Number:35604-67-2
- Molecular formula:C13H20ClNO3
- Molecular Weight:273.7558
94-71-3
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35604-67-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / tert-butyl methyl ether / 48 h / 45 °C
2.1: toluene / 6 h / Reflux
3.1: sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride / toluene / 0.17 h / 20 °C
3.2: 20 - 40 °C
4.1: hydrogenchloride; hydrogen / palladium on activated charcoal / ethanol / 2 h / 60 °C
References:
Supernus Pharmaceuticals Inc. US2011/251198, 2011, A1
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35604-67-2
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$118.00/100mg