4-(1,3-dioxoisoindolin-2-yl)-N-(thiazol-2-yl)benzenesulfonamide synthesis
- Product Name:4-(1,3-dioxoisoindolin-2-yl)-N-(thiazol-2-yl)benzenesulfonamide
- CAS Number:36340-59-7
- Molecular formula:C17H11N3O4S2
- Molecular Weight:385.42
Yield:36340-59-7 92%
Reaction Conditions:
with acetic acid at 120;
Steps:
4.1. General procedure A: Synthesis of phthalimide derivatives (1a-1c)
General procedure: The compounds were prepared through condensation reaction between 0.001 mol phthalic anhydride and 0.001 mol sulfonamides in 10 mL acetic acid under reflux at 120 °C for 3-4 h. Then 20 mL distilled water was added into the reaction media. The compounds were filtered and recrystallized in ethanol.30
References:
Akgün, Hülya;Karamelekoglu, Irem;Berk, Barkin;Kurnaz, I?il;Saribiyik, Gizem;?ktem, Sinem;Kocag?z, Tanil [Bioorganic and Medicinal Chemistry,2012,vol. 20,# 13,p. 4149 - 4154] Location in patent:experimental part
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