4,4',4'',4'''-silanetetrayltetrabenzaldehyde synthesis
- Product Name:4,4',4'',4'''-silanetetrayltetrabenzaldehyde
- CAS Number:1055999-34-2
- Molecular formula:C28H20O4Si
- Molecular Weight:448.54
24856-58-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -65 °C / Inert atmosphere
1.2: 870 min / -65 - 20 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; water / 2 h / Reflux
References:
WO2022/254902,2022,A1