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4,4,5,5,6,6,6-HEPTAFLUOROHEXAN-1-OL synthesis

2synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 87 percent / azoisobutyronitrile (AIBN), Bu₃SnH / 55 - 65 °C
2: 91 percent / aq NaOH / 3 h / Heating

References:

Larsson, Ulf;Carlson, Rolf;Leroy, Jacques [Acta Chemica Scandinavica,1993,vol. 47,# 4,p. 380 - 390]

Perfluorohexanoic acid 2-(Perfluorobutyl)ethyl acrylate (NONAFLUORO-N-BUTYL)EPOXIDE PERFLUOROHEXALDEHYDE HYDRATE 3-PERFLUOROBUTYL-1,2-EPOXYPROPANE

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