4,4'-DINITRODIPHENYL ETHER synthesis
- Product Name:4,4'-DINITRODIPHENYL ETHER
- CAS Number:101-63-3
- Molecular formula:C12H8N2O5
- Molecular Weight:260.2
582-25-2
367 suppliers
$5.00/25g
350-46-9
528 suppliers
$10.60/1gm:
101-63-3
124 suppliers
$10.00/1g
Yield:101-63-3 98.5%
Reaction Conditions:
with sodium carbonate in ISOPROPYLAMIDE
Steps:
7 EXAMPLE 7
EXAMPLE 7 A 250 ml flask equipped with an agitator, thermometer, and nitrogen bleed is charged with 66.5 (0.47 mole) p-fluoronitrobenzene, 77 g dimethylacetamide, 0.57 g (0.004 mole) potassium benzoate and 25 g (0.24 mole) sodium carbonate. The reaction mixture is heated to and maintained at 170° C. while it is agitated and kept under a nitrogen blanket. After 12 hours 4,4'-dinitrodiphenyl ether is obtained in 98.5% yield.
References:
E. I. Du Pont de Nemours and Company US4558164, 1985, A
100-00-5
70 suppliers
$14.00/25g
101-63-3
124 suppliers
$10.00/1g
1146127-11-8
10 suppliers
$114.00/1g
24067-17-2
259 suppliers
$19.00/1g
101-63-3
124 suppliers
$10.00/1g
905718-45-8
24 suppliers
$23.30/25MG
101-63-3
124 suppliers
$10.00/1g