4,6,8-trimethylquinolin-2-ol synthesis
- Product Name:4,6,8-trimethylquinolin-2-ol
- CAS Number:42414-28-8
- Molecular formula:C12H13NO
- Molecular Weight:187.24
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / tetrahydrofuran; water / 16 h / Reflux
2.1: triethylamine / dichloromethane / 25 °C / Inert atmosphere
2.2: 25 °C
3.1: (4-fluorophenyl)-λ3-iodanediyl diacetate / chloroform / 24 h / 25 °C / Sealed tube
References:
Fan, Huaqiang;Pan, Peng;Zhang, Yongqiang;Wang, Wei [Organic Letters,2018,vol. 20,# 24,p. 7929 - 7932]