4,7-Dichloro-1-indanone synthesis
- Product Name:4,7-Dichloro-1-indanone
- CAS Number:52977-63-6
- Molecular formula:C9H6Cl2O
- Molecular Weight:201.05
29682-41-5
136 suppliers
$7.00/5g
52977-63-6
37 suppliers
$72.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 94 percent / Et3N; Pd(OAc)2 / acetonitrile / 1 h / 110 °C
2: 95 percent / H2 / PtO2 / ethyl acetate / 24 h / 20 °C
3: SOCl2 / 4 h / Heating
4: 1.001 g / AlCl3 / CS2 / 24 h / Heating
References:
Zhou, Zhang-Lin;Kher, Sunil M.;Cai, Sui Xiong;Whittemore, Edward R.;Espitia, Stephen A.;Hawkinson, Jon E.;Tran, Minhtam;Woodward, Richard M.;Weber, Eckard;Keana, John F. W. [Bioorganic and Medicinal Chemistry,2003,vol. 11,# 8,p. 1769 - 1780]
20595-47-5
73 suppliers
$59.00/5g
52977-63-6
37 suppliers
$72.00/100mg
68034-76-4
42 suppliers
$23.00/100mg
52977-63-6
37 suppliers
$72.00/100mg