4-ACETAMIDO-2-METHYLNITROBENZENE synthesis
- Product Name:4-ACETAMIDO-2-METHYLNITROBENZENE
- CAS Number:51366-39-3
- Molecular formula:C9H10N2O3
- Molecular Weight:194.19
611-05-2
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75-36-5
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$17.92/100G
51366-39-3
60 suppliers
$403.00/500mg
Yield:51366-39-3 97%
Reaction Conditions:
with pyridine in dichloromethane at 0 - 20; for 3 h;
Steps:
1
Compound 20-3 (0429) To a solution of Pyridine (20 mL) and AcCl (6.158 g, 78.947) in DCM (100 mL) was added the solution of 20-2 (10 g, 65.789 mmol) in pyridine (20 mL) at 0° C. The mixture was stirred at room temperature for 3 h. The volatiles were removed under reduced pressure and the residue was washed with water (100 mL×3), dried under reduced pressure to afford 20-3 as yellow solid (12.5 g, yield: 97%).
References:
US9138427,2015,B2 Location in patent:Page/Page column 297
537-92-8
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$10.00/1g
51366-39-3
60 suppliers
$403.00/500mg
7418-36-2
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90868-29-4
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108-24-7
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$14.00/250ML
108-44-1
378 suppliers
$9.00/1g
51366-39-3
60 suppliers
$403.00/500mg
7418-36-2
5 suppliers
inquiry
90868-29-4
4 suppliers
inquiry
537-92-8
123 suppliers
$10.00/1g
51366-39-3
60 suppliers
$403.00/500mg
611-05-2
162 suppliers
$16.00/1g
108-24-7
0 suppliers
$14.00/250ML
51366-39-3
60 suppliers
$403.00/500mg