4-ACETAMIDOBENZYLAMINE synthesis
- Product Name:4-ACETAMIDOBENZYLAMINE
- CAS Number:25412-53-7
- Molecular formula:C9H12N2O
- Molecular Weight:164.2
35704-19-9
131 suppliers
$12.00/5g
25412-53-7
31 suppliers
inquiry
Yield:25412-53-7 96%
Reaction Conditions:
Stage #1: N-(4-cyanophenyl)acetamidewith cobalt(III) acetylacetonate;tris(2-(dicyclohexylphosphanyl)ethyl)phosphane in tert-butyl alcohol;Sealed tube;Inert atmosphere;
Stage #2: with potassium tert-butylate in tert-butyl alcohol;Sealed tube;Inert atmosphere;
Stage #3: with hydrogen in tert-butyl alcohol at 80; under 22502.3 Torr; for 18 h;Autoclave;
References:
Adam, Rosa;Bheeter, Charles Beromeo;Cabrero-Antonino, Jose R.;Junge, Kathrin;Jackstell, Ralf;Beller, Matthias [ChemSusChem,2017,vol. 10,# 5,p. 842 - 846]
122-85-0
234 suppliers
$10.00/1g
25412-53-7
31 suppliers
inquiry