4-Aminomethylquinoline hydrochloride synthesis
- Product Name:4-Aminomethylquinoline hydrochloride
- CAS Number:5632-13-3
- Molecular formula:C10H10N2
- Molecular Weight:158.2
2973-27-5
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5632-13-3
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Yield:5632-13-3 94%
Reaction Conditions:
with hydrogen in dichloromethane at 35; under 775.743 Torr; for 0.75 h;
Steps:
1.7 Catalytic modification of QCN
General procedure: The Pd/AC was synthesized as per our reported procedure using Pd(NO3)2 solution (Chanotiya et al. 2016). Surface area was measured using Beckman Coulter SA3100 surface area analyser. Surface area of the Pd/AC catalyst is 380 sqm/g. Mettler Toledo TGA/DSC1 Stare system was used for the thermo-gravimetric analysis (Dhiman et al. 2017). The TGA-DTG analysis of this catalyst inferred that there was no major weight loss in the temperature range of 50-800oC. Therefore the catalyst was stable in this temperature range mentioned above. TEM CM 200 of Philips make used for the transmission electron microscope analysis with operating voltage 20-200 kv of 2.4Ao resolution. Isolated QCN was further reduced using Pd/Ac catalyst at different temperature and solvent systems (Table S3). In another approach, the reduced products having similar structural relationship with QCN, so this compound is further confirmed through derivatization.
References:
Rout, Prasant Kumar;Kumar, Prashant;Rao, Y. Ramachandra;Kumar, Anant;Bawankule, Dnyaneshwar U.;Singh, Ruchi;Singh, Kijay Bahadur;Chanotiya, Chandan Singh;Naik [Natural Product Research,2021,vol. 35,# 10,p. 1632 - 1638] Location in patent:supporting information
126921-64-0
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5632-13-3
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491-35-0
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5632-13-3
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4363-93-3
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5632-13-3
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3964-04-3
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5632-13-3
75 suppliers
$82.79/250 mg