4-(Benzyloxy)-2-butanol synthesis
- Product Name:4-(Benzyloxy)-2-butanol
- CAS Number:4799-69-3
- Molecular formula:C11H16O2
- Molecular Weight:180.24
774-44-7
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4799-69-3
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Yield:4799-69-3 83%
Reaction Conditions:
Stage #1: 4-methyl-2-phenyl-[1,3]dioxanewith 9-borabicyclo[3.3.1]nonane dimer in toluene; for 18 h;Inert atmosphere;Reflux;
Stage #2: with ethanolamine in toluene at 20; for 1 h;Inert atmosphere;
References:
Soderquist, John A.;Kock, Iveliz;Estrella, Maria E. [Organic Process Research and Development,2006,vol. 10,# 5,p. 1076 - 1079] Location in patent:supporting information