4-BENZYLOXY-3-METHYLBENZOIC ACID synthesis
- Product Name:4-BENZYLOXY-3-METHYLBENZOIC ACID
- CAS Number:72323-93-4
- Molecular formula:C15H14O3
- Molecular Weight:242.27
1439364-88-1
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Yield:-
Reaction Conditions:
with water;sodium hydroxide in methanol;
Steps:
37
Likewise, intermediate 98 was prepared from 94 in two steps following similarexperimental conditions as described for the preparation of 47. Analytical data forintermediate 98: 1H-NMR (400 MHz, DMSO-d6): ? 12.51 (br s, 1H), 7.75-7.77 (m, 2H), 7.46-7.48 (m, 2H), 7.38-7.42 (m, 2H), 7.33-7.35 (m, 1 H), 7.08 (d, J=8.0 Hz, 1 H), 5.20 (5, 2H) and 2.22 (5, 3H). LC-MS: 241 .05 (M-H).
References:
WO2018/165718,2018,A1 Location in patent:Page/Page column 100; 102
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