ChemicalBook CAS DataBase List 4-Chloro-2-fluorotoluene

4-Chloro-2-fluorotoluene synthesis

1synthesis methods

Product Name:4-Chloro-2-fluorotoluene
CAS Number:452-75-5
Molecular formula:C7H6ClF
Molecular Weight:144.57

148839-33-2
167 suppliers
$6.00/1g

452-75-5
257 suppliers
$16.00/25 g

Yield:452-75-5 11.9 mg

Reaction Conditions:

Stage #1:(5-chloro-2-methylphenyl)boronic acid with C₂₇H₂₃N₄O₆PdS;potassium carbonate in methanol;benzene at 23; for 10 h;
Stage #2: with Selectfluor in acetonitrile at 50; for 0.5 h;

References:

Furuya, Takeru;Kaiser, Hanns Martin;Ritter, Tobias [Angewandte Chemie - International Edition,2008,vol. 47,# 32,p. 5993 - 5996] Location in patent:supporting information; experimental part

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4-Chloro-2-fluorotoluene synthesis

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